摘要:目的:建立HPLC法同时测定银翘解毒片中绿原酸、连翘酯苷A、木犀草苷及牛蒡苷含量的方法。方法:反向高效液相色谱法,色谱柱:月旭柱(Uitimate XB-C18柱4.6mm×250mm,5μm);流动相:乙腈(A)-0.4%磷酸水(B),梯度洗脱,流速:1.0mL/min;检测波长:280nm、330nm。结果:绿原酸、连翘苷A、木犀草苷和牛蒡苷的回归方程分别是Y=1527834X-6507、Y=1050567X-10859、Y=1269219X-9026、Y=744039X-11568,它们分别在0.243~4.861μg、0.155~3.093μg、0.029~0.578μg、0.185~3.701μg范围内线性关系良好,相关系数R2=0.999 4~0.999 6,加样回收率分别为98.42%,98.74%、99.734%和98.79%,RSD分别为1.68%,1.52%、2.18%和1.22%。结论:本文所建立的银翘解毒片4个指标成分同时定量的方法准确、可靠,可作为银翘解毒片质量控制的参考方法。
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